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S4R InertBridge™ — Vacuum Transfer Chamber for Air-Sensitive SEM Samples

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The S4R InertBridge™ is a compact vacuum transfer chamber developed for the protected transfer of air-sensitive samples from a glovebox to a scanning electron microscope. Samples remain enclosed within an evacuated compartment during handling and transport, limiting their exposure to ambient oxygen, moisture, and laboratory contamination.

The chamber is evacuated and closed inside the glovebox. Under ambient conditions, the pressure differential across the cover maintains contact with the sealing interface. Once the InertBridge™ is installed inside the SEM and the microscope chamber is pumped down, the external pressure progressively decreases. When the resulting closing force becomes lower than the force exerted by the integrated spring mechanism, the cover moves laterally to expose the samples for observation.

The standard sample holder provides four Ø8 mm positions with a nominal position geometry of Ø8 × 0.5 mm. Alternative sample-holder geometries can be configured according to the intended samples and experimental workflow. A machine-specific SEM mounting adapter is included, with configurations available for selected ZEISS, JEOL, and Thermo Scientific platforms, as well as other microscope models following compatibility review.

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Vacuum Transfer Chamber for Air-Sensitive Samples

S4R InertBridge™

Protected Glovebox-to-SEM Transfer for Air- and Moisture-Sensitive Samples

The S4R InertBridge™ is a compact vacuum transfer chamber developed for the protected transfer of air-sensitive samples from a glovebox to a scanning electron microscope.

A pressure-differential retention mechanism maintains the cover against the sealing interface during handling and transport, while an integrated spring drives its lateral opening during SEM pump-down.

Sample Capacity
4 Positions
Standard Sample Recess
Ø8 mm × 0.5 mm deep
Nominal Mass
200 g
SEM Integration
Model-Specific Adapter
Product Highlights

Protected transfer through a compact pressure-responsive system

Designed to limit atmospheric exposure between controlled sample preparation in a glovebox and observation inside a scanning electron microscope.

01
Protected Transfer
Maintains air-sensitive samples inside an evacuated compartment during transfer from the glovebox to the SEM.
02
Pressure-Differential Retention
The pressure difference between the evacuated sample compartment and ambient atmosphere retains the cover against the sealing interface.
03
Pressure-Responsive Opening
During SEM pump-down, the decreasing external pressure releases the cover and allows the integrated spring to drive its lateral opening.
04
Configurable Integration
Machine-specific mounting adapters and alternative sample-holder geometries can be configured for the intended experimental setup.
Operating Workflow

Protected transfer from glovebox preparation to SEM observation

The complete procedure is carried out through six clearly defined steps, from sample preparation under controlled atmosphere to pressure-responsive sample exposure inside the SEM chamber.

01
Inside the Glovebox

Sample Preparation

Prepare and position the samples in the four-position sample holder under the required controlled-atmosphere conditions.

02
Inside the Glovebox

Chamber Loading

Insert the loaded sample holder into the InertBridge™ sample compartment and place the cover in its closing position.

03
Inside the Glovebox

Evacuation and Closure

Evacuate the sample compartment. The resulting pressure differential retains the cover against the sealing interface.

04
Protected Transfer

Glovebox-to-SEM Transfer

Remove the closed chamber from the glovebox and carry it to the SEM. The sample compartment remains sealed during handling and transfer.

05
SEM Integration

SEM Installation

Install the InertBridge™ in the microscope using the dedicated model-specific SEM mounting adapter.

06
Pressure-Responsive Release

SEM Pump-Down and Opening

As SEM chamber pressure decreases, the retaining force diminishes until the spring drives the cover laterally and exposes the samples.

Operating principle: pressure-differential retention keeps the chamber closed during transfer. SEM pump-down reduces the retaining force and enables spring-driven lateral opening.
02
Pressure-Responsive Opening

Passive release during SEM chamber evacuation

During transport under ambient laboratory pressure, the pressure outside the evacuated sample compartment is higher than the pressure inside it. The resulting pressure differential generates a net retaining force that holds the cover against the sealing interface.

As the SEM chamber is evacuated, the external pressure decreases and the net retaining force across the cover progressively diminishes. Once this force falls below the preload of the integrated spring mechanism, the cover is released and moves laterally to expose the samples.

Ambient Transfer
Cover Maintained Closed
SEM Pump-Down
Closing Force Decreases
Sample Exposure
Spring-Driven Opening
Passive operating principle
The release sequence depends on the pressure differential, the effective cover area, the sealing interface, and the spring preload. No powered actuator is required inside the SEM chamber.
03
Sample Holder

Four-position holder with configurable sample-recess geometry

The standard InertBridge™ sample holder incorporates four cylindrical sample recesses. Each recess has a nominal diameter of Ø8 mm and a nominal depth of 0.5 mm.

Because the intended specimens are solid, the recess diameter and depth are the most relevant dimensional specifications. Alternative holder layouts can be evaluated according to the sample geometry and analytical workflow.

Standard Capacity
4 Samples
Standard Recess
Ø8 mm × 0.5 mm deep
Custom Layouts
Available
Configuration service
Custom sample-holder development is based on the sample dimensions, required number of positions, mounting method, available microscope clearance, and intended analysis conditions.
04
SEM Integration

Model-specific integration across SEM platforms

The InertBridge™ is installed inside the microscope through a dedicated mounting adapter configured for the specified SEM model. One compatible mounting adapter is included according to the selected product configuration.

Adapter configurations are available for selected ZEISS, JEOL, and Thermo Scientific SEM models. Compatibility must be confirmed for the exact microscope model and stage configuration. Other platforms can be evaluated according to the mechanical interface, chamber clearance, stage geometry, and cover-opening envelope.

Selected ZEISS, JEOL, and Thermo Scientific SEM models
Model-specific adapters can be configured for selected instruments from these manufacturers. Compatibility is confirmed for the exact microscope model supplied by the customer.
Confirm the exact SEM model before ordering
Please contact S4R with the exact microscope model and stage configuration. Compatibility depends on the mounting interface, available chamber volume, detector arrangement, working-distance requirements, and cover-opening direction.
Typical Applications

SEM characterization of air- and moisture-sensitive materials

Intended for mounted samples whose surface chemistry, morphology, or analytical response may be altered by exposure to ambient oxygen or moisture.

Battery Materials and Interfaces
Protected transfer of prepared electrodes, interfacial cross sections, and other mounted battery materials for SEM imaging and compatible microanalysis.
Solid Electrolytes
Transfer of moisture-sensitive or reactive solid-electrolyte materials following preparation under controlled atmosphere.
Air-Sensitive Functional Materials
Protected transfer of mounted functional materials whose surfaces may oxidize, hydrate, or otherwise change rapidly when exposed to laboratory air.
Mounted Powders, Thin Films, and Cross Sections
Protected transfer of secured powder specimens, crystals, thin films, cross sections, and other mounted samples prepared under controlled atmosphere.
Dimensions and Mass

Compact geometry for SEM chamber integration

Refer to the dimensional drawing for the external envelope, mounting interface, sample position, and lateral cover-opening clearance.

Nominal Chamber Mass
200 g
External Dimensions
See Dimensional Drawing
Technical Specifications

S4R InertBridge™ Specifications

Parameter Specification
Product Type Vacuum transfer chamber for air-sensitive samples intended for SEM analysis
Primary Transfer Route Glovebox to scanning electron microscope
Sample-Protection Principle Transfer inside an evacuated, closed sample compartment
Closure Principle Pressure-differential retention against the sealing interface
Opening Principle Pressure-responsive release with spring-driven lateral opening
Cover Movement Spring-driven lateral opening
Powered In-Chamber Actuator Not required
Standard Sample Capacity 4 sample positions
Standard Sample-Recess Geometry 4 cylindrical recesses, each Ø8 mm × 0.5 mm deep
Custom Sample Holder Alternative geometries available upon request
Nominal Chamber Mass 200 g
External Dimensions Refer to the dimensional drawing
SEM Mounting Interface Model-specific mounting adapter
Standard Platform Families Selected ZEISS, JEOL, and Thermo Scientific SEM models; exact model confirmation required
Other SEM Platforms Custom integration available following compatibility review
SEM Adapter One compatible mounting adapter included according to the selected configuration
Positioning Stand Dedicated positioning stand included
Vacuum Pump Available as an option
Intended Operating Environment Controlled-atmosphere sample loading followed by transfer to an SEM vacuum chamber
06
Included Components

Complete transfer chamber configuration

Transfer Chamber
Complete InertBridge™ chamber with cover, sealing interface, opening mechanism, and vacuum connection
Sample Holder
Standard four-position sample holder with four cylindrical recesses, each Ø8 mm × 0.5 mm deep
Positioning Stand
Dedicated positioning stand for stable positioning during sample loading, chamber evacuation, and routine handling
SEM Adapter
One machine-specific mounting adapter configured for the validated SEM platform
Documentation
User manual covering sample loading, evacuation, transport, SEM installation, operation, and handling
Optional Equipment
Optional vacuum pump package for pre-evacuation of the sample compartment
Microscope configuration
The exact SEM model and mounting interface must be communicated before ordering so that the appropriate adapter and opening orientation can be confirmed.
Protection-performance note: Transfer performance depends on the initial evacuation level, the condition and cleanliness of the sealing interface, transport duration, and correct handling of the chamber.
SEM-compatibility note: Compatibility is not determined by the microscope brand alone. The exact SEM model, stage interface, chamber clearance, detector geometry, required working distance, sample height, and lateral cover-opening envelope must be reviewed before final adapter validation.

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